CSC Scientific Blog

A blog about test equipment

CSC Scientific Blog

Loss On Drying Moisture Analysis and Other Moisture Mysteries II Vapor Pressure

Posted by Art Gatenby on Nov 22, 2010 5:55:00 PM

A while ago on these pages I agonized about loss-on-drying moisture analysis . As you may recall, my explorations of the drying process overwhelmed me with evaporation concepts , vapor pressure notions, water content complexities and water activity witchcraft, all just to dry something.
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Topics: Evaporation, Moisture Analysis, Moisture Testing, Loss-On-Drying

Having Trouble Performing a duNouy Ring Test in Thick Samples?

Posted by Art Gatenby on Nov 15, 2010 3:29:00 PM

My musings were interrupted this week with a pressing challenge. It was stated like this:

 “My duNouy ring kept falling off the arm hook when attempting to immerse it into a high-viscosity sample.”

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Topics: duNouy Rings, Surface Tension Measurement, Surface Tension, Interfacial Tensiometer, tensiometers

Is Particle-Size Analysis Boring? Trivial? Amazing? Exciting? Vital?

Posted by Art Gatenby on Nov 2, 2010 3:57:00 PM

When I tell people at cocktail parties that we specialize in Particle-Size Analysis. I usually get a polite response of ------ “OH !!,”   which translates to “So who cares?”

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Topics: Sonic Sifter, Particle Size Analysis, Sieves, Sieving Process

Loss-On-Drying Moisture Analysis and Other Moisture Mysteries I

Posted by Art Gatenby on Oct 25, 2010 3:52:00 PM

One quiet night, I was musing over moisture analysis and how easy it is to do using loss-on drying. Little did I know what was in store.

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Topics: Moisture Analysis, Moisture Testing, Loss-On-Drying

Surface Tension by duNouy Rings or Wilhelmy Plates – Which to Choose?

Posted by Art Gatenby on Aug 19, 2010 5:16:00 PM

When tempted to think I know all there is about surface tension measurement, further information brings me back to earth. I’m conversant with the principal applications: surfactant analysis, plating, detecting contaminants, development of ink and the like. I have assisted customers to set up and calibrate duNouy Ring tensiometers for most applications -- all the while taking for granted that the Ring technique was the method of choice -- with only infrequent questions arising about Wilhelmy Plate tensiometers.

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Topics: Wilhelmy Plates, duNouy Rings, Tensiometer, Surface Tension

Certify Sieves or Calibrate Sieves --- Should You Do It?

Posted by Art Gatenby on Jun 30, 2010 4:57:00 PM

The relative value of a sieve certification process vs a sieve calibration has perplexed me for a long time.

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Topics: Sieve Shakers, Mid-Point Sieves, Particle Size Analysis, Sieve Calibration, Sieve Testing, Sieves

View from Inside a Karl Fischer Titration Cell.

Posted by Art Gatenby on May 17, 2010 4:26:00 PM

 When people are looking for a way to measure small amounts of moisture, we often recommend the Karl Fischer method.

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Topics: Karl Fischer, Karl Fischer Titration

Static Electricity and Sieves: No Problem -- Maybe

Posted by Art Gatenby on Apr 21, 2010 2:02:00 PM

I'll bet that most of you have experienced the shock of walking on a thick wool rug on a dry winter's day and getting zapped out of your reverie when reaching for the metal door knob.

The same process of static electricity generation can play havoc with your sieving process.

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Topics: Sieve Blinding, Agglomeration, Sieve Testing, Sieves

Is My Test Equipment Lying?

Posted by Art Gatenby on Mar 9, 2010 4:45:00 PM

I keep running into this kind of thing.

There is a recurring question we are asked as instrument manufacturers:

"Is my equipment working OK?"

This is of particular concern when a production process seems to be off standard.

QC says: "Clearly Process Problems"

Production says: "Bad Test Results"

These challenges arise often.

What to do?

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Topics: Surface Tension

Re-Certify Mid-Point Sieves? When and How?

Posted by Art Gatenby on Jan 29, 2010 12:24:00 PM

I recently had a long conversation with the person [we'll call him Bill] responsible for setting up the quality procedures for very tight specifications in a new process -- part of which was developing procedures for checking the ongoing tolerances of production sieves.
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Topics: Mid-Point Sieves, Sieve Calibration, Sieve Testing, Sieves

Is Your Moisture Test Result Really Moisture?

Posted by Art Gatenby on Jan 11, 2010 11:22:00 AM

Most of us think about measuring moisture by...

  1. Drying the material and measure the weight loss 
  2. Using a calibration and electronic instrument 
  3. Using a titration method such as Karl Fischer

When using these processes, we take for granted that the results will be the product's actual moisture.

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Topics: Moisture Oven Test, Infrared Moisture, Moisture Analysis, Moisture Testing, Karl Fischer Titration, Loss-On-Drying

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